Experiment name: Dyeing of cotton fabric with sulphur dyes.
Introduction:
Sulpher dye is a popular dyes for dyeing of black shade and its advantage is cost effective. Its water insoluble and converted to a water soluble from having affinity for cellulose.
Objective:
- To learn about dyeing process of cotton fabric with sulpher dye.
- To dye cotton fabric by sulpher dye.
Machine & Materials:
- Sample dyeing machine.
- Oven dryer.
- Biker.
- sample fabric cotton.
- Measuring Cylinder.
- Pipette.
Recipe:
Wetting agent =0.5 g/l (1% s.s)Sequestering agent =1 g/l (1% s.s)
Sulpher dye =2% (2% s.s)
Sodium sulphide =3 g/l(1% s.s)
Glauber salt =10 g/l (2% s.s)
Soda ash =1 g/l (1% s.s)
Time =1 hour
Temperature = 90 degree
M:L =1:20
Sample Weight =5 gm
Calculation:
Total liquor =5*20=100 mlRequire dye =Shad % weight of fabric in gm / stock solution
=2%*5 gm/2%
=5 gm
wetting agent=(0.5*5*20*100/1000*1)
=5 ml
sequestering agent=10 ml
sodium sulphide=30 ml
glauber salt= 10 gm
soda ash=10 ml
process sequence:
- Collection of cotton fabric .
- Reduction at 80 degree for 10 min.
- Dyeing with sulpher dye.
- Physical oxidation.
- Cold rinsing .
- Hot wash.
- Cold rinsing.
- Drying.
thank you
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